1. Kukhona amakristalu aphezulu-conductivity kuseli conductivity.
Isixazululo: Ngemva kokuhlanza i-conductivity cell nge-1:1 nitric acid, yigeze ngamanzi enziwe deionized.
2. I-event ayihlanzekile ngokwanele.
Isixazululo: shintsha umbala.
3. Ikholomu ye-chromatographic imunca izinto ezine-conductivity ephezulu.
Isixazululo: Washcolumn ngokuphindaphindiwe futhi ngokushintshana nge-eluent namanzi.
4. Ukukhetha okungalungile kwesikali sokulinganisa
Lapho kwenziwa ukuhlaziya ama-ions avumayo, njengoba i-conductivity yangemuva ye-eluate iphezulu kakhulu, ukukhethwa kwesikali sokulinganisa esiphansi kakhulu kuzoholela ekubonisweni kwevelu ye-conductivity ephezulu kakhulu.Vele ukhethe isikali sokulinganisa futhi.
5. Umcindezeli akasebenzi
Isixazululo: Hlola ukuthi isicindezeli sivuliwe yini.
6. Ukugxiliswa kwesampula kuphezulu kakhulu.
Isixazululo: Nciphisa isampula.
1. Kunamabhamuza empompini.
Isixazululo: Ivalvu yokukhipha ekhipha amandla ehambisana newashi yevalvu yokukhipha umoya yepompo, amabhamuza aqeda amandla.
2. I-valve yokuhlola yepompo ingcolile noma yonakele.
Isixazululo: Shintsha i-valve yokuhlola noma uyibeke kusixazululo se-nitric esingu-1:1 sokuhlanza okunamandla.
3. Isihlungi ebhodleleni le-eluent singcolile noma sivinjiwe.
Isixazululo: Faka esikhundleni isihlungi.
4. Ukukhipha umoya okwanele kwe-eluent.
Isixazululo: Faka esikhundleni i-eluent.
Isixazululo: Hlola indawo yokuvala eduze kwendlela yokugeleza ukuze ubone futhi ususe ukuvala.
1. I-membrane yesihlungi sekholomu ivinjiwe.
Isixazululo: Khipha ikholomu futhi ukhulule isiphetho sokungena.Khipha ipuleti yesisefo ngokucophelela, yifake ku-1:1 nitric acid bese uyigeza ngegagasi le-ultrasonic imizuzu engu-30, bese uyihlanza ngamanzi e-deionized bese uyihlanganisela emuva, buyisela emuva ukuhlanganisa i-chromatograph ukuze ihlanjululwe.Qaphela ukuthi i-chromatograph ayikwazi ukuxhunywa nendlela yokugeleza.
2. Ivalvu yomjovo wezindlela eziyisithupha ivimbekile.
Isixazululo: Hlola indawo evalekile ngalapho kugeleza khona ukuze ubone futhi uxazulule.
3. I-valve yokuhlola yepompo ivinjiwe.
Isixazululo: Shintsha i-valve yokuhlola noma uyibeke kusixazululo se-nitric esingu-1:1 sokuhlanza okunamandla.
4. Umzila ogelezayo uvinjelwe.
Isixazululo: thola indawo yokuvala ngokusho kwendlela yokususa kancane kancane bese wenza enye indawo.
5. Isivinini esidlulele.
Isixazululo: Lungisa iphampu ibe nezinga lokugeleza elifanele.
6. Ingcindezi ephezulu yomkhawulo wepompo isethwe iphansi kakhulu.
Isixazululo: Ngaphansi kokugeleza komsebenzi wekholomu ye-chromatographic, lawula ukucindezela komkhawulo okuphezulu kakhulu ukuze kube ngu-5 MPa ngaphezu kwengcindezi yamanje yokusebenza.
1. Idivayisi ayisebenzi isikhathi eside ngokwanele njengoba bekuhleliwe.
Isixazululo:Ukufakwa okuqhubekayo kwe-eluent kuze kube yilapho izinsimbi zizinzile.
2. Kunamabhamuza empompini.
Isixazululo: Ivalvu yokukhipha ekhipha amandla ehambisana newashi yevalvu yokukhipha umoya yepompo, amabhamuza aqeda amandla.
3. Isihlungi sepayipi lokungena kwamanzi lepompo livinjiwe, likhiqize ukucindezela okungalungile ngaphansi kwamandla okudonsa kanye nokukhiqiza amabhamuza.
Isixazululo: Ukushintsha isihlungi noma ukubeka isihlungi ku-1:1 1M i-nitric acid ezowashwa 5min ngokugeza kwe-ultrasonic.
4. Kunamabhamuza kukholamu.
Isixazululo: Sebenzisa i-eluent elungiselelwe ngamanzi ahlukanisiwe ukuze uhlanza ikholomu ngesivinini esiphansi ukuze ususe amabhamuza.
5. Kunamabhamuza endleleni yokugeleza.
Isixazululo: Susa ikholomu bese ukhipha amabhamuza emanzini.
6. Kunamabhamuza kuseli conductivity, okubangela ukushintshashintsha njalo kwesisekelo.
Isixazululo: I-flushing conductivity cel, amabhamuza aqeda amandla
7. I-voltage ayizinzile noma iphazamisekile i-electrostatic static.
Isixazululo: Faka i-voltage stabilizer bese ugaya insimbi.
1. Isikhathi sokushisisa ngaphambilini socingo asanele.
Isixazululo: Nweba isikhathi sokushisisa kwangaphambili.
2. Ukuvuza kokugeleza.
Isixazululo: thola indawo evuzayo futhi uyilungise, uma ingenakuxazululeka, buyisela isihlanganisi.
3. I-voltage ayizinzile noma iphazamisekile i-static electrostatic.
Isixazululo: Faka i-voltage stabilizer bese ugaya insimbi.
1. Ukugxila kwe-eluent akulungile.
Isixazululo: Khetha ukugxilisa ingqondo efanele .
2. Izinga lokugeleza kwe-eluentis liphezulu kakhulu.
Isixazululo: Khetha isilinganiso esifanele sokugeleza kwe-eluent.
3. Ukusebenzisa amasampula anokugxilisa ingqondo ngokweqile
Isixazululo: Nciphisa isampula.
4. Ikholomu ingcolile.
Isixazululo: Khiqiza kabusha noma shintsha ikholomu.
1. Umthamo womjovo wesampula awushintshi.
Isixazululo: Jova isampula ngevolumu izikhathi ezingaphezu kweziyi-10 zevolumu yeringi ukuze uqinisekise umjovo ogcwele.
2. Ukugxila kwesampula elijovwe akufanelekile.
Isixazululo: Khetha ukugxiliswa okufanele kwesampula elijovwe.
3. I-reagent ayihlanzekile.
Isixazululo: Faka esikhundleni i-reagent.
4. Izinto zangaphandle zikhona emanzini ase-deionized.
Isixazululo: Faka esikhundleni samanzi enziwe deionized.
5. Ukugeleza kuyashintsha.
Isixazululo: Thola izizathu zalolo shintsho bese ulungisa isimo sangempela.
6. Umzila wokugeleza uvinjelwe.
Isixazululo: thola indawo evinjiwe, lungisa noma wenze enye.
1. I-reagent ayihlanzekile.
Isixazululo: Faka esikhundleni ama-reagents.
2. Amanzi acwebile aqukethe ukungcola.
Isixazululo: Faka esikhundleni samanzi enziwe deionized.
1. Ukufakwa okungalungile kweseli conductivity.
Isixazululo: Faka kabusha iseli conductivity.
2. Iseli ye-conductivity conductivity ilimele.
Isixazululo: Faka esikhundleni iseli conductivity.
3. Iphampu ayinaso isisombululo sokuphumayo.
Isixazululo: Hlola inkomba yokucindezela ukuze uqinisekise ukuthi iphampu iyasebenza yini.
1. Isixazululo esijwayelekile singcolisiwe, ikakhulukazi amasampula angagxili kakhulu.
Isixazululo: Lungisa kabusha ikhambi.
2. Amanzi acwebile angcolile.
Isixazululo: buyisela amanzi e-deionized.
3. Ukugxiliswa kwesampula kuphezulu kakhulu noma kuphansi kakhulu, ngaphandle komugqa womugqa wedivayisi.
Isixazululo: Khetha uhla olufanele lokugxilisa ingqondo.
Isixazululo: buyisela intambo kagesi noma ukunikezwa kwamandla okungashintshi.
1. Igesi emuncwa epayipini lomzila wokugeleza
Isixazululo: lapho ukunikezwa kwamanzi kuvuliwe, vula ivalve yokukhipha umoya yepompo, qalisa iphampu ye-plunger futhi uhlale udlidliza isihlungi ukuze uyikhiphe ngokugcwele igesi.
2. Izinga lokushisa langaphakathi eliphezulu kakhulu eliholela ekukhishweni kwegesi okunganele kwamanzi enziwe i-deionized.
Isixazululo: Sebenzisa idivayisi yokukhipha umoya eku-inthanethi.
3. I-valve yokuhlola yepompo ingcolile noma yonakele.
Isixazululo: Shintsha i-valve yokuhlola noma uyibeke kusixazululo se-nitric esingu-1:1 sokuhlanza okunamandla.